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Formation of Aluminum-Doped Zinc Oxide Nanocrystals via the Benzylamine Route at Low Reaction Kinetics

Ungerer, J.; Thurm, A.-K.; Garnweitner, G.; Nirschl, H.

Abstract:
The influence of essential process parameters on the adjustability of specific process and particulate properties of aluminum‐doped zinc oxide (AZO) nanocrystals during synthesis via the benzylamine route at low reaction kinetics is demonstrated by enabling time‐resolved access of the selected measurement technique. It is shown that the validity of the pseudo‐first‐order process kinetics could be extended to the minimum operable reaction kinetics. On the other hand, the impacts of the process temperature and the initial precursor concentration on both the process kinetics and the particle morphology are discussed. The obtained data provide a versatile tool for precise process control by adjusting defined application‐specific particle properties of AZO during synthesis.

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Verlagsausgabe §
DOI: 10.5445/IR/1000118222
Veröffentlicht am 17.07.2020
Originalveröffentlichung
DOI: 10.1002/ceat.201900466
Scopus
Zitationen: 2
Web of Science
Zitationen: 1
Cover der Publikation
Zugehörige Institution(en) am KIT Institut für Mechanische Verfahrenstechnik und Mechanik (MVM)
Publikationstyp Zeitschriftenaufsatz
Publikationsjahr 2020
Sprache Englisch
Identifikator ISSN: 0930-7516, 1521-4125
KITopen-ID: 1000118222
Erschienen in Chemical engineering & technology
Verlag Wiley
Band 43
Heft 5
Seiten 797-803
Vorab online veröffentlicht am 07.02.2020
Nachgewiesen in Web of Science
Scopus
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