KIT | KIT-Bibliothek | Impressum | Datenschutz

X-ray diffraction and thermoanalytical datasets of precursors of the Gd$_{6}$UO$_{12-δ}$ phase processed by combined mechanochemical−thermal routes

Darin, Gaspar; Imakuma, Kengo; Santiago, Rafael Trautwein; Da Silva, Klebson Lucenildo; Cótica, Luiz Fernardo; Fabián, Martin; Valíček, Jan; Hahn, Horst; Šepelák, Vladimír

Abstract:
The datasets presented here are related to the research paper entitled “Disordered Gd$_{6}$UO$_{12-δ}$ with the cation antisite defects prepared by a combined mechanochemical−thermal method”. The datasets complement the findings on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid precursors (3Gd$_{2}$O$_{3}$ + UO$_{2}$) on the formation of Gd$_{6}$UO$_{12-δ}$ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd$_{2}$O$_{3}$ + UO$_{2}$ mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd$_{2}$O$_{3}$ + UO$_{2}$ mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated 3Gd$_{2}$O$_{3}$ + UO$_{2}$ mixture measured in air at a heat rate of 10 K/min.


Verlagsausgabe §
DOI: 10.5445/IR/1000139493
Veröffentlicht am 28.10.2021
Originalveröffentlichung
DOI: 10.1016/j.dib.2021.106972
Cover der Publikation
Zugehörige Institution(en) am KIT Institut für Nanotechnologie (INT)
Publikationstyp Zeitschriftenaufsatz
Publikationsmonat/-jahr 04.2021
Sprache Englisch
Identifikator ISSN: 2352-3409
KITopen-ID: 1000139493
HGF-Programm 43.31.01 (POF IV, LK 01) Multifunctionality Molecular Design & Material Architecture
Erschienen in Data in Brief
Verlag Elsevier
Band 35
Seiten Art.-Nr.: 106972
Nachgewiesen in Scopus
KIT – Die Forschungsuniversität in der Helmholtz-Gemeinschaft
KITopen Landing Page