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Revealing the mechanism of reductive, mechanochemical Li recycling from LiFePO4

Geiß, David ORCID iD icon 1; Dolotko, Oleksandr 1; Indris, Sylvio ORCID iD icon 1; Neemann, Christian 1; Bologa, Andrei 1; Bergfeldt, Thomas ORCID iD icon 2; Knapp, Michael ORCID iD icon 1; Ehrenberg, Helmut 1
1 Institut für Angewandte Materialien – Energiespeichersysteme (IAM-ESS), Karlsruher Institut für Technologie (KIT)
2 Institut für Angewandte Materialien – Angewandte Werkstoffphysik (IAM-AWP), Karlsruher Institut für Technologie (KIT)


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Zugehörige Institution(en) am KIT Institut für Angewandte Materialien – Angewandte Werkstoffphysik (IAM-AWP)
Institut für Angewandte Materialien – Energiespeichersysteme (IAM-ESS)
Publikationstyp Forschungsdaten
Publikationsdatum 16.05.2024
Erstellungsdatum 31.01.2024 - 31.01.2024
Identifikator DOI: 10.35097/1912
KITopen-ID: 1000167962
HGF-Programm 38.02.03 (POF IV, LK 01) Batteries in Application
Lizenz Creative Commons Namensnennung 4.0 International
Liesmich

X-ray powder diffraction (XRD): Data was processed using WinXPow to transform the obtained .raw data into .xy data avoiding negative intensities. Data was plotted using OriginLab.
57Fe Mössbauer spectroscopy: The spectra were fitted with WinNormos and plotted using OriginLab.
X-ray absorption spectroscopy (XAS): All XAS spectra were analyzed and processed utilizing the ATHENA software package. The X-ray absorption near edge spectra (XANES) regions of the XAS spectra were acquired by subtracting the pre-edge background from the overall absorption and normalizing to the spline fit using the ATHENA software package.
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